3,5-二氯-N-[(1-乙基吡咯烷-2-基)甲基]-2,6-二甲氧基苯甲酰胺合成路线 （共 4 条）
反应条件
thionyl chloride in diethyl ether; water; toluene
参考文献
Astra Lakemedel Aktiebolag
Patent: US4232037 A1, 1980 ;
US 4232037 A
反应条件
1: 60 percent / SO2Cl2 / CHCl3 / 0.5 h / Heating
2: SOCl2 / 0.23 h / Heating
3: butan-2-one / 2 h / Ambient temperature
View Scheme
参考文献
Florvall, Lennart; Oegren, Sven-Ove
Journal of Medicinal Chemistry, 1982 , vol. 25, # 11 p. 1280 - 1286
反应条件
1: SOCl2 / 0.23 h / Heating
2: butan-2-one / 2 h / Ambient temperature
View Scheme
参考文献
Florvall, Lennart; Oegren, Sven-Ove
Journal of Medicinal Chemistry, 1982 , vol. 25, # 11 p. 1280 - 1286
反应条件
in butanone
2 h; Ambient temperature; Yield given;
参考文献
Florvall, Lennart; Oegren, Sven-Ove
Journal of Medicinal Chemistry, 1982 , vol. 25, # 11 p. 1280 - 1286
