反应条件
1: 6.5 g / aq. acetic acid / 2 h / Heating
2: 4.3 g / 3percent KOH / methanol / 2.5 h
3: 3.7 g / pyridinium tosylate / tetrahydrofuran / 24 h / Ambient temperature
4: n-BuLi / tetrahydrofuran; hexane / 1 h / Heating
5: 270 mg / n-BuLi / tetrahydrofuran; hexane / 2 h / Ambient temperature
6: pyridinium tosylate / methanol / 20 h / Ambient temperature
7: cyclohexanone, aluminium isopropoxide / toluene / 0.5 h / Heating
View Scheme
参考文献
Marcotte; Robinson
Steroids, 1982 , vol. 39, # 3 p. 325 - 344