E-P,P-二苯基-N-(1-苯基亚乙基)膦酰胺合成路线 (共 33 条)
反应条件
1: With sodium tetrahydridoaluminate; (-)-(R,R)-TADDOL in tetrahydrofuran T=-70°C; 2: With hydrogenchloride in methanol T=20°C; 3 h; Title compound not separated from byproducts;
参考文献
Vinogradov; Gorshkova; Chel'tsova; Pavlov; Razmanov; Ferapontov; Malyshev; Heise
Russian Chemical Bulletin, 2003 , vol. 52, # 2 p. 471 - 479
反应条件
potassium tert-butylate in benzene 4 h; Ambient temperature;
参考文献
Kobayashi; Kakiuchi; Kato
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 2 p. 392 - 395
反应条件
potassium tert-butylate; benzaldehyde 1) C6H6, r.t., 10 min., 2) C6H6, 2 h, r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kobayashi; Kakiuchi; Kato
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 2 p. 392 - 395
反应条件
potassium tert-butylate 1) C6H6, r.t., 10 min., 2) C6H6, 2 h, r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kobayashi; Kakiuchi; Kato
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 2 p. 392 - 395
反应条件
1: NaBH4+tetrahydrofurfuryl alcohol / (S,S)-Co(II) complex catalyst (C48H54N2O4Co) / ethanol; CHCl3 / 4 h / 0 °C 2: HCl / methanol / 3 h / 25 °C View Scheme
参考文献
Sugi, Kiyoaki D.; Nagata, Takushi; Yamada, Tohru; Mukaiyama, Teruaki
Chemistry Letters, 1997 , # 6 p. 493 - 494
反应条件
1: With sodium tetrahydridoaluminate; (-)-(R,R)-TADDOL in tetrahydrofuran T=-70°C; 2: With hydrogenchloride in methanol T=20°C; 3 h; Title compound not separated from byproducts;
参考文献
Vinogradov; Gorshkova; Chel'tsova; Pavlov; Razmanov; Ferapontov; Malyshev; Heise
Russian Chemical Bulletin, 2003 , vol. 52, # 2 p. 471 - 479
反应条件
potassium tert-butylate; benzaldehyde 1) C6H6, r.t., 10 min., 2) C6H6, 2 h, r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 2 p. 392 - 395
反应条件
potassium tert-butylate 1) C6H6, r.t., 10 min., 2) C6H6, 2 h, r.t.; Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 2 p. 392 - 395
反应条件
potassium tert-butylate 1) C6H6, r.t., 10 min., 2) C6H6, 2 h, r.t.; Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 2 p. 392 - 395
反应条件
potassium tert-butylate 1) C6H6, r.t., 10 min., 2) C6H6, 2 h, r.t.; Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 2 p. 392 - 395