3-(1,3-二氧杂烷-2-基)丙醛合成路线 （共 7 条）
反应条件
magnesium in tetrahydrofuran
1.5 h; Ambient temperature;
参考文献
Lucchesini, Francesco
Tetrahedron, 1992 , vol. 48, # 45 p. 9951 - 9966
反应条件
pyridinium chlorochromate in dichloromethane
T=23°C; Oxidation; 3 h;
参考文献
Shiu, Lin-Hun; Li, Yang-Lian; Li, Chien-Le; Lao, Ching-Yu; Chen, Wei-Chen; Yu, Chin-Hui; Liu, Rai-Shung
Journal of Organic Chemistry, 1999 , vol. 64, # 20 p. 7552 - 7558
反应条件
1: With ozone in dichloromethane
T=-78°C;
2: With triphenylphosphine in dichloromethane
T=-78 - 20°C;
参考文献
Schenkel, Laurie B.; Ellman, Jonathan A.
Organic Letters, 2004 , vol. 6, # 20 p. 3621 - 3624
反应条件
bis[(S,S,S)-DiazaPhos-SPE]; [rhodium(I)(carbonyl)2(acetylacetonate)]; hydrogen in tetrahydrofuran; toluene
T=40°C; P=8000.32 Torr; 4 h; optical yield given as percent eeenantioselective reaction;
参考文献
McDonald, Richard I.; Wong, Gene W.; Neupane, Ram P.; Stahl, Shannon S.; Landis, Clark R.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14027 - 14029
反应条件
1: 57 percent / LiAlH4 / diethyl ether / 2 h / Heating
2: 55 percent / pyridinium chlorochromate, NaOAc / CH2Cl2 / 2 h
View Scheme
参考文献
Herdewijn, Piet; Claes, Paul J.; Vanderhaeghe, Hubert
Journal of Medicinal Chemistry, 1986 , vol. 29, # 5 p. 661 - 664
反应条件
1: Mg / tetrahydrofuran / 1 h
2: tetrahydrofuran / 1.5 h
View Scheme
参考文献
Tsuie, Barbara; Reddinger, Jerry L.; Sotzing, Gregory A.; Soloducho, Jadwiga; Katritzky, Alan R.; Reynolds, John R.
Journal of Materials Chemistry, 1999 , vol. 9, # 9 p. 2189 - 2200
反应条件
in tetrahydrofuran
Carbonylation; 1.5 h;
参考文献
Tsuie, Barbara; Reddinger, Jerry L.; Sotzing, Gregory A.; Soloducho, Jadwiga; Katritzky, Alan R.; Reynolds, John R.
Journal of Materials Chemistry, 1999 , vol. 9, # 9 p. 2189 - 2200
