2,2-二甲基-5-乙氧羰基-1,3-二氧六环合成路线 （共 6 条）
反应条件
lithium aluminium tetrahydride in diethyl ether 2.5 h; Ambient temperature;
参考文献
Dubois, Joelle; Foures, Christine; Bory, Sonia; Falcou, Serge; Gaudry, Michel; Marquet, Andree
Tetrahedron, 1991 , vol. 47, # 6 p. 1001 - 1012
反应条件
sodium chloride in dimethyl sulfoxide
T=180°C; 24 h;
参考文献
Iwata; Maezaki; Hattori; Fujita; Moritani; Takemoto; Tanaka; Imanishi
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 2 p. 339 - 345
反应条件
1: 89 percent / p-toluenesulfonic acid monohydrate / 5 h / Ambient temperature
2: 74 percent / aq. NaCl / dimethylsulfoxide / 24 h / 180 °C
View Scheme
参考文献
Iwata; Maezaki; Hattori; Fujita; Moritani; Takemoto; Tanaka; Imanishi
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 2 p. 339 - 345
反应条件
sodium chloride in water; dimethyl sulfoxide
6 h; Heating;
参考文献
Dubois, Joelle; Foures, Christine; Bory, Sonia; Falcou, Serge; Gaudry, Michel; Marquet, Andree
Tetrahedron, 1991 , vol. 47, # 6 p. 1001 - 1012
反应条件
toluene-4-sulfonic acid; sodium chloride
2.) DMSO, H2O, 180 deg C; Yield given. Multistep reaction;
参考文献
Iwata, Chuzo; Fujita, Masahiro; Moritani, Yasunori; Sugiyama, Kenji; Hattori, Kohji; Imanishi, Takeshi
Tetrahedron Letters, 1987 , vol. 28, # 27 p. 3131 - 3134
反应条件
Yield given. Multistep reaction;
参考文献
Dubois, Joelle; Foures, Christine; Bory, Sonia; Falcou, Serge; Gaudry, Michel; Marquet, Andree
Tetrahedron, 1991 , vol. 47, # 6 p. 1001 - 1012
