单(2-乙基-6-羟基己基)邻苯二甲酸酯合成路线 （共 3 条）
反应条件
1: With diborane in tetrahydrofuran
T=0 - 20°C;
2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran
T=50°C; 1 h;
参考文献
Nuti, Francesca; Hildenbrand, Sibylle; Chelli, Mario; Wodarz, Roman; Papini, Anna Maria
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 10 p. 3461 - 3465
反应条件
1.1: 94 percent / pyridine / 3 h / Heating
2.1: B2H6 / tetrahydrofuran / 0 - 20 °C
2.2: 89 percent / NaOH; H2O2 / tetrahydrofuran / 1 h / 50 °C
View Scheme
参考文献
Nuti, Francesca; Hildenbrand, Sibylle; Chelli, Mario; Wodarz, Roman; Papini, Anna Maria
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 10 p. 3461 - 3465
反应条件
1.1: 94 percent / pyridine / 3 h / Heating
2.1: B2H6 / tetrahydrofuran / 0 - 20 °C
2.2: 89 percent / NaOH; H2O2 / tetrahydrofuran / 1 h / 50 °C
View Scheme
参考文献
Nuti, Francesca; Hildenbrand, Sibylle; Chelli, Mario; Wodarz, Roman; Papini, Anna Maria
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 10 p. 3461 - 3465
