反应条件
potassium hydroxide; iodine in diethyl ether; dimethyl sulfoxide addn. of C6H5CH(COOC2H5)2 to mixt. of Cr(CO)3-complex/powd. KOH in DMSO (stirring; 20°C, 6 h), diln. with aq. HCl, extn. with Et2O, treating with excess I2 (room temp., 3 h); distn. (reduced pressure); identification by GC and NMR;
参考文献
Baldoli, Clara; Buttero, Paola Del; Licandro, Emanuela; Maiorana, Stefano
Gazzetta Chimica Italiana, 1988 , vol. 118, # 5 p. 409 - 414
