2,4,6-三羟基苯甲酸合成路线 （共 56 条）
反应条件
1: With potassium carbonate in acetone
2: With boron trichloride in dichloromethane
T=-78°C;
参考文献
Napolitano, Carmela; McArdle, Patrick; Murphy, Paul V.
Journal of Organic Chemistry, 2010 , vol. 75, # 21 p. 7404 - 7407
反应条件
1: diethyl ether
2: diethyl ether
3: diethyl ether
View Scheme
参考文献
Bielitza, Max; Pietruszka, Joerg
Chemistry - A European Journal, 2013 , vol. 19, # 25 p. 8300 - 8308
参考文献
Balgir,B.S. et al.
Australian Journal of Chemistry, 1973 , vol. 26, p. 2459 - 2472
反应条件
1: potassium carbonate / acetone / 20 °C / |Molecular sieve
2: boron trichloride / dichloromethane; n-heptane / 1 h / -78 - 20 °C
3: trichlorophosphate / acetonitrile / 0 - 20 °C / |Inert atmosphere
View Scheme
参考文献
Bielitza, Max; Pietruszka, Joerg
Chemistry - A European Journal, 2013 , vol. 19, # 25 p. 8300 - 8308
反应条件
air; methylene blue in methanol
10 h; Irradiation; Product distributionMechanism;
参考文献
Chibber, S. S.; Dutt, S. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 352 - 353
反应条件
1: phosphoryl chloride; zinc chloride
2: diethyl ether; methanol
View Scheme
参考文献
Shah; Shah
Journal of Scientific and Industrial Research, 1956 , vol. 15 B, p. 630,632
