1: 1,3-dihydro-1-oxo-2H-indene With lithium hexamethyldisilazane in tetrahydrofuran
T=0 - 20°C; 0.333333 h;
2: TFETFA in tetrahydrofuran
T=20°C; 0.333333 h;
3: With ammonium chloride in tetrahydrofuran; water
参考文献
Riofski, Mark V.; John, Jinu P.; Zheng, Mary M.; Kirshner, Julia; Colby, David A.
Journal of Organic Chemistry, 2011 , vol. 76, # 10 p. 3676 - 3683
1: With magnesium in diethyl ether
T=0 - 20°C; Grignard reaction;
2: With toluene-4-sulfonic acid in benzene
Heating;
参考文献
Grimmer, Neil E.; Coville, Neil J.; De Koning, Charles B.; Smith, Jeremy M.; Cook, Leanne M.
Journal of Organometallic Chemistry, 2000 , vol. 616, # 1-2 p. 112 - 127
ALPHA CHEM CO., LTD.; NAM, Hyun Goog; LIM, Dae Won; KIM, Jae Yong; PARK, Sang Mi; JANG, Seung Hee; LEE, Sang Youn; HAM, Ju Seok; CHO, Kyu Oh; KIM, Hyun Don
Patent: WO2013/180376 A1, 2013 ;
Location in patent: Paragraph 191; 192; 193 ;
