2-羟基-1,4-萘醌合成路线 （共 313 条）
反应条件
in ethanol
T=150°C; 0.333333 h; Microwave irradiation;
参考文献
Sharma, Abhinay; Santos, Isabela O.; Gaur, Pratibha; Ferreira, Vitor F.; Garcia, Celia R.S.; Da Rocha, David R.
European Journal of Medicinal Chemistry, 2013 , vol. 59, p. 48 - 53
反应条件
in ethanol
T=150°C; 0.333333 h; Microwave irradiation;
参考文献
Sharma, Abhinay; Santos, Isabela O.; Gaur, Pratibha; Ferreira, Vitor F.; Garcia, Celia R.S.; Da Rocha, David R.
European Journal of Medicinal Chemistry, 2013 , vol. 59, p. 48 - 53
反应条件
di-tert-butyl peroxide
7 h; Heating;
参考文献
Boehm, Peter; Cooper, Kelvin; Hudson, Alan T.; Elphick, Jane P.; McHardy, Nicholas
Journal of Medicinal Chemistry, 1981 , vol. 24, # 3 p. 295 - 299
反应条件
di-tert-butyl peroxide
7 h; Heating;
参考文献
Boehm, Peter; Cooper, Kelvin; Hudson, Alan T.; Elphick, Jane P.; McHardy, Nicholas
Journal of Medicinal Chemistry, 1981 , vol. 24, # 3 p. 295 - 299
反应条件
dimethylsulfide borane complex
1.) THF, reflux, 3 h, 2.) THF, H2O, 20 min; Yield given. Multistep reaction;
参考文献
Boehm, Peter; Cooper, Kelvin; Hudson, Alan T.; Elphick, Jane P.; McHardy, Nicholas
Journal of Medicinal Chemistry, 1981 , vol. 24, # 3 p. 295 - 299
反应条件
1: 9 percent / silver oxide / CHCl3
2: 1) dithionite, 2) NaOH / 1) ether
3: 92 percent / H2 / Pd/C / methanol; benzene / 40 °C
View Scheme
参考文献
Laaatsch
1983 , vol. NO. 11, p. 1886 - 1900
反应条件
formaldehyd; ethanol
参考文献
Dalgliesh
Journal of the American Chemical Society, 1949 , vol. 71, p. 1697,1700
反应条件
acetic acid; Petroleum ether
T=90°C;
参考文献
Fieser et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 3177
参考文献
Baltzer
Chemische Berichte, 1881 , vol. 14, p. 1902
反应条件
acetic acid in water
T=100°C; 12 h;
参考文献
Nakanishi; Nakajima; Sato; Ozawa; Tohda; Umezawa
Analytical Chemistry, 2001 , vol. 73, # 13 p. 2920 - 2928
