2-羟基-1,4-萘醌合成路线 （共 313 条）
反应条件
in dichloromethane 0.0833333 h; Heating;
参考文献
Molecules, , vol. 10, # 1 p. 226 - 237
反应条件
oxygen; sodium hydroxide in methanol T=0°C; 2.5 h;
参考文献
Catalysis Letters, , vol. 141, # 12 p. 1808 - 1813
反应条件
trifluoroacetic acid T=0°C; 0.25 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 12 p. 4048 - 4050
反应条件
hydrogenchloride T=120°C;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 154, p. 307
反应条件
boron tribromide in dichloromethane 2 h; Ambient temperature;
参考文献
Inoue, Kenichiro; Ueda, Shinichi; Nayeshiro, Hidekazu; Moritome, Nobuharu; Inouye, Hiroyuki
Phytochemistry (Elsevier), 1984 , vol. 23, # 2 p. 313 - 318
反应条件
1: 1.8 g / O2, K / 2-methyl-propan-2-ol / 4 h / Ambient temperature 2: 1.0 g / conc. HCl / 3 h / Heating 3: 1.) SnCl2, conc. HCl; 2.) 50percent KOH / 1.) EtOH, r.t., 1 h; 2.) reflux, 1 h 4: 2 mg / NaBH4, PdCl2 / methanol / 1 h / Ambient temperature 5: 393 mg / BBr3 / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 23, # 2 p. 313 - 318
反应条件
1: SOCl2 / 1 h / Heating 2: AlCl3 / CS2 / 3 h / Heating 3: 1.8 g / O2, K / 2-methyl-propan-2-ol / 4 h / Ambient temperature 4: 1.0 g / conc. HCl / 3 h / Heating 5: 1.) SnCl2, conc. HCl; 2.) 50percent KOH / 1.) EtOH, r.t., 1 h; 2.) reflux, 1 h 6: 2 mg / NaBH4, PdCl2 / methanol / 1 h / Ambient temperature 7: 393 mg / BBr3 / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 23, # 2 p. 313 - 318
反应条件
1: 1.0 g / conc. HCl / 3 h / Heating 2: 1.) SnCl2, conc. HCl; 2.) 50percent KOH / 1.) EtOH, r.t., 1 h; 2.) reflux, 1 h 3: 2 mg / NaBH4, PdCl2 / methanol / 1 h / Ambient temperature 4: 393 mg / BBr3 / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 23, # 2 p. 313 - 318
反应条件
1: AlCl3 / CS2 / 3 h / Heating 2: 1.8 g / O2, K / 2-methyl-propan-2-ol / 4 h / Ambient temperature 3: 1.0 g / conc. HCl / 3 h / Heating 4: 1.) SnCl2, conc. HCl; 2.) 50percent KOH / 1.) EtOH, r.t., 1 h; 2.) reflux, 1 h 5: 2 mg / NaBH4, PdCl2 / methanol / 1 h / Ambient temperature 6: 393 mg / BBr3 / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 23, # 2 p. 313 - 318
反应条件
1: 1.) SnCl2, conc. HCl; 2.) 50percent KOH / 1.) EtOH, r.t., 1 h; 2.) reflux, 1 h 2: 2 mg / NaBH4, PdCl2 / methanol / 1 h / Ambient temperature 3: 393 mg / BBr3 / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 23, # 2 p. 313 - 318
