2,4,6-三甲氧基苯甲醛合成路线 （共 65 条）
参考文献
PIRAMAL LIFE SCIENCES LIMITED; BANDGAR, Babasaheb Pandurang; TOTRE, Jalindar Vasant
Patent: WO2011/121505 A1, 2011 ;
Location in patent: Page/Page column 42 ;
反应条件
K2OsO2(OH)4; chloramine-T in water; tert-butyl alcohol 0.416667 h; chemoselective reaction;
参考文献
Devari, Shekaraiah; Deshidi, Ramesh; Kumar, Manjeet; Kumar, Arvind; Sharma, Simmi; Rizvi, Masood; Kushwaha, Manoj; Gupta, Ajai Prakash; Shah, Bhahwal Ali
Tetrahedron Letters, 2013 , vol. 54, # 48 p. 6407 - 6410
反应条件
1: phloroglucinol trimethyl ether With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 2 h; 3: methanol Further stages;
参考文献
Tetrahedron, , vol. 68, # 24 p. 4701 - 4709
反应条件
1: With aluminium trichloride in toluene T=20°C; 15 h; 2: With water in toluene T=20°C; 2 h; Further stages.;
参考文献
Tobisu, Mamoru; Yamaguchi, Seiji; Chatani, Naoto
Organic Letters, 2007 , vol. 9, # 17 p. 3351 - 3353
反应条件
trichlorophosphate T=40 - 50°C; Vilsmeier reaction;
参考文献
Gallardo-Godoy, Alejandra; Fierro, Angelica; McLean, Thomas H.; Castillo, Mariano; Cassels, Bruce K.; Reyes-Parada, Miguel; Nichols, David E.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 7 p. 2407 - 2419
反应条件
silver trifluoromethanesulfonate in dichloromethane T=0°C; 0.25 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 78, # 7 p. 3438 - 3444
反应条件
AlCl3, aluminium chloride in chlorobenzene T=0 - 18°C; 22 h;
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 63, # 4 p. 395 - 406
反应条件
in sulfuric acid 1 h;
参考文献
Panda; Parthasarathy
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 7 p. 628 - 631
反应条件
in sulfuric acid 1 h;
参考文献
Panda; Parthasarathy
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 7 p. 628 - 631
反应条件
1: 68 percent / POCl3 / 6 h / Heating 2: 65 percent / H2SO4 / 1 h View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 40, # 7 p. 628 - 631
