2,4,6-三甲氧基苯甲醛合成路线 （共 65 条）
反应条件
hydrogenchloride 0.333333 h; 150 deg C -> 120 deg C;
参考文献
Rappoport, Zvi; Apeloig, Yitzhak; Greenblatt, Jeremy
Journal of the American Chemical Society, 1980 , vol. 102, # 11 p. 3837 - 3848
反应条件
1: in diethyl ether T=-78 - 20°C; 2: With triethylsilane; trifluoroacetic acid in dichloromethane T=-78 - 20°C;
参考文献
Roelens, Frederik; Heldring, Nina; Dhooge, Willem; Bengtsson, Martin; Comhaire, Frank; Gustafsson, Jan-Ake; Treuter, Eckardt; De Keukeleire, Denis
Journal of Medicinal Chemistry, 2006 , vol. 49, # 25 p. 7357 - 7365
反应条件
CuF2 in water; dimethyl sulfoxide T=120°C; 12 h; Schlenk techniqueInert atmosphereGreen chemistry;
参考文献
Li, Pan; Zhao, Jingjing; Lang, Rui; Xia, Chungu; Li, Fuwei
Tetrahedron Letters, 2014 , vol. 55, # 2 p. 390 - 393
反应条件
1: alkali; KMnO4 2: methanolic potash View Scheme
参考文献
Herzig; Wenzel; Gehringer
Monatshefte fuer Chemie, 1903 , vol. 24, p. 866
反应条件
tert.-butylhydroperoxide; copper(l) chloride in acetonitrile T=20°C; 1.5 h;
参考文献
Mannam, Sreedevi; Sekar
Tetrahedron Letters, 2008 , vol. 49, # 6 p. 1083 - 1086
反应条件
sodium formate; N-(2-amino-ethyl)-4-methyl-benzenesulphonamide; [{(η5-C5Me5)IrCl}2(μ-Cl)2] T=80°C; 1.5 h;
参考文献
Wu, Xiaofeng; Liu, Jianke; Li, Xiaohong; Zanotti-Gerosa, Antonio; Hancock, Fred; Vinci, Daniele; Ruan, Jiwu; Xiao, Jianliang
Angewandte Chemie - International Edition, 2006 , vol. 45, # 40 p. 6718 - 6722
参考文献
Freudenberg; Harder
Justus Liebigs Annalen der Chemie, 1927 , vol. 451, p. 222
反应条件
boron tribromide in dichloromethane T=-78 - 20°C; 1.5 h;
参考文献
Roelens, Frederik; Huvaere, Kevin; Dhooge, Willem; Van Cleemput, Marjan; Comhaire, Frank; De Keukeleire, Denis
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 10 p. 1042 - 1051
反应条件
cerium(III) chloride; sodium iodide in acetonitrile dealkylation; 9 h; Heating;
参考文献
Chemistry Letters, , # 7 p. 738 - 739
反应条件
Rhodium trichloride; 1,3-bis-(diphenylphosphino)propane in diethylene glycol dimethyl ether 40 h; Heating;
参考文献
Advanced Synthesis and Catalysis, , vol. 348, # 15 p. 2148 - 2154
