1-溴-2-(1,1,2,2-四氟乙氧基)苯合成路线 (共 6 条)
反应条件
1: phenol With potassium hydroxide in methanol Metallation; 2: 1,2-dibromo-1,1,2,2-tetrafluoroethane in dimethyl sulfoxide T=60°C; Etherification; 6 h;
参考文献
Journal of Fluorine Chemistry, , vol. 105, # 1 p. 129 - 135
反应条件
caesium carbonate in dimethyl sulfoxide T=50°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 48, # 42 p. 7516 - 7519
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide 6 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 25, # 43 p. 4937 - 4940
参考文献
Journal of Materials Chemistry, , vol. 16, # 15 p. 1470 - 1474
反应条件
K3PO4*3H2O in N,N-dimethyl-formamide T=80°C; 90 h; Inert atmosphere;
参考文献
Zhang, Cheng-Pan; Chen, Qing-Yun; Xiao, Ji-Chang; Gu, Yu-Cheng
Journal of Fluorine Chemistry, 2009 , vol. 130, # 7 p. 671 - 673
反应条件
zinc in acetonitrile
Heating;
参考文献
Zhang, Sen; Liu, Hao; Deng, Yan; Huang, Xiaoyu
Journal of Fluorine Chemistry, 2012 , vol. 133, p. 184 - 189