1: 90 percent / SCl2 / various solvent(s); CCl4 / 0.25 h / 40 °C 2: various solvent(s); CCl4 / 1.5 h / Heating 3: 97 percent / CH2Cl2 / 4 h / Ambient temperature 4: 90 percent / NaOH / hexane; H2O 5: 100 percent / 2,2,4-trimethyl-pentane / 0.25 h / Heating 6: 28 percent / methanol / 3 h / Irradiation View Scheme

1: 90 percent / SCl2 / various solvent(s); CCl4 / 0.25 h / 40 °C 2: various solvent(s); CCl4 / 1.5 h / Heating 3: 97 percent / CH2Cl2 / 4 h / Ambient temperature 4: 90 percent / NaOH / hexane; H2O 5: 100 percent / 2,2,4-trimethyl-pentane / 0.25 h / Heating 6: 5 percent / Raney-Nickel (W5) / ethanol / 4 h / Heating View Scheme