1-(1,3-苯并二氧戊环-5-基)-2-氯乙酮合成路线 (共 6 条)
反应条件
bromine; toluene-4-sulfonic acid in dichloromethane 48 h;
参考文献
Antunes, Heidi; Fardelone, Lucidio C.; Rodrigues, J. Augusto R.; Moran, Paulo J.S.
Tetrahedron Asymmetry, 2004 , vol. 15, # 17 p. 2615 - 2620
反应条件
sulfuryl dichloride in dichloromethane
T=0°C; 1.5 h;
参考文献
Antunes, Heidi; Fardelone, Lucidio C.; Rodrigues, J. Augusto R.; Moran, Paulo J.S.
Tetrahedron Asymmetry, 2004 , vol. 15, # 17 p. 2615 - 2620
反应条件
hydrogenchloride
T=0°C;
参考文献
Chatterjea, J. N.; Shaw, S. C.; Fatma, A.
Journal of the Indian Chemical Society, 1985 , vol. 62, p. 990 - 992
反应条件
1: thionyl chloride / benzene / 4 h / Heating
2: diethyl ether
3: HCl / 0 °C
View Scheme
参考文献
Chatterjea, J. N.; Shaw, S. C.; Fatma, A.
Journal of the Indian Chemical Society, 1985 , vol. 62, p. 990 - 992
反应条件
1: diethyl ether
2: HCl / 0 °C
View Scheme
参考文献
Chatterjea, J. N.; Shaw, S. C.; Fatma, A.
Journal of the Indian Chemical Society, 1985 , vol. 62, p. 990 - 992
反应条件
bromine; toluene-4-sulfonic acid in dichloromethane
48 h;
参考文献
Antunes, Heidi; Fardelone, Lucidio C.; Rodrigues, J. Augusto R.; Moran, Paulo J.S.
Tetrahedron Asymmetry, 2004 , vol. 15, # 17 p. 2615 - 2620