7-(1-环庚-2,4,6-三烯基)环庚-1,3,5-三烯合成路线 (共 29 条)
反应条件
1,1'-diethylene-2,2'-bipyridinium ion in acetonitrile
IrradiationThe reduction of tropylium cation with the concomitant oxidation of O,O'-dialkyldithiophosphate anion (dtp-) by visible irradiation, in the presence of diquat cation; MechanismProduct distribution;
参考文献
Deronzier, Alain
Tetrahedron Letters, 1984 , vol. 25, # 27 p. 2867 - 2868
反应条件
chloranil in benzene
3 h; Irradiation; Product distribution;
参考文献
Mori, Akira; Takeshita, Hitoshi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 5 p. 1581 - 1584
反应条件
in tetrahydrofuran; hexane; N,N-dimethyl-formamide
T=-78°C;
参考文献
Bauer, Walter; Daub, Joerg
Tetrahedron Letters, 1982 , vol. 23, # 46 p. 4773 - 4776
反应条件
in benzene
Ambient temperatureIrradiationI2-CCl4 filter solution, 340-420 nm;
参考文献
Kondo, Hirosato; Mori, Masato; Kanematsu, Ken
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5273 - 5278
反应条件
n-butyllithium
1.) -78 deg C, THF, 1h 2.) THF, 0 deg C, 1h; Yield given. Multistep reaction;
参考文献
Badejo, Ibraheem T.; Karaman, Rafik; Pinkerton, A. Alan; Fry, James L.
Journal of Organic Chemistry, 1990 , vol. 55, # 14 p. 4327 - 4332
反应条件
chromium powder in hydrogenchloride; water
T=25°C;
参考文献
Takeuchi, Ken'ichi; Kurosaki, Takeshi; Yokomichi, Yasunori; Kimura, Yoshihiro; Kubota, Yasuhiro; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 670 - 674
反应条件
in toluene
1 h; Heating;
参考文献
Mori, Akira; Mametsuka, Hiroaki; Takeshita, Hitoshi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 7 p. 2072 - 2077
参考文献
Menzek, Abdullah; Kazaz, Cavit; Eryigit, Feryat; Cengiz, Mustafa
Journal of Chemical Research, 2004 , # 3 p. 210 - 212
反应条件
in toluene
1.5 h; Heating;
参考文献
Mori, Akira; Mametsuka, Hiroaki; Takeshita, Hitoshi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 7 p. 2072 - 2077
反应条件
T=120°C; 1.5 h; Further byproducts given;
参考文献
Mori, Akira; Mametsuka, Hiroaki; Takeshita, Hitoshi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 7 p. 2072 - 2077