1: Ph(CH2)2OBn With 1-bromo-1,1-dimethylethane; [C5mim](+)*Br(-) T=60°C; 2: thiophenol With [C5mim](+)*Br(-) T=60°C; Title compound not separated from byproducts;
参考文献
Advanced Synthesis and Catalysis, , vol. 347, # 14 p. 1811 - 1818
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反应条件
in toluene soln. of Ti complex treated with PhCH2Br, refluxed with stirring under N2 for 4.5 h; evapn. to dryness (rotatory evaporator) upon cooling, extn. (hexanes), filtration (insol. Cp2TiBr2), evapn. of the filtrate;
