1,2-去氢-N-乙酰基多巴胺合成路线 （共 5 条）
反应条件
boron tribromide in dichloromethane
T=-60°C; Yield given;
参考文献
Ramamurthy, B.; Sugumaran, M.
Synthesis, 1987 , # 5 p. 523 - 524
反应条件
1: thionyl chloride / benzene / 2 h / Heating
2: sodium azide / acetone; H2O / 1 h / 0 °C
3: benzene / 4 h / Heating
4: diethyl ether; tetrahydrofuran / 2 h / 0 °C
5: boron tribromide / CH2Cl2 / -60 °C
View Scheme
参考文献
Ramamurthy, B.; Sugumaran, M.
Synthesis, 1987 , # 5 p. 523 - 524
反应条件
1: sodium azide / acetone; H2O / 1 h / 0 °C
2: benzene / 4 h / Heating
3: diethyl ether; tetrahydrofuran / 2 h / 0 °C
4: boron tribromide / CH2Cl2 / -60 °C
View Scheme
参考文献
Ramamurthy, B.; Sugumaran, M.
Synthesis, 1987 , # 5 p. 523 - 524
反应条件
1: diethyl ether; tetrahydrofuran / 2 h / 0 °C
2: boron tribromide / CH2Cl2 / -60 °C
View Scheme
参考文献
Ramamurthy, B.; Sugumaran, M.
Synthesis, 1987 , # 5 p. 523 - 524
反应条件
1: benzene / 4 h / Heating
2: diethyl ether; tetrahydrofuran / 2 h / 0 °C
3: boron tribromide / CH2Cl2 / -60 °C
View Scheme
参考文献
Ramamurthy, B.; Sugumaran, M.
Synthesis, 1987 , # 5 p. 523 - 524
