表没食子儿茶素 3-O-(3-O-甲基)没食子酸酯合成路线 （共 4 条）
反应条件
hydrogen; palladium dihydroxide in tetrahydrofuran; methanol
T=20°C; 6 h;
参考文献
Wan, Sheng Biao; Ping Dou; Chan, Tak Hang
Tetrahedron, 2006 , vol. 62, # 25 p. 5897 - 5904
反应条件
caesium carbonate; thiophenol in acetonitrile
T=0 - 20°C; Inert atmosphere;
参考文献
Aihara, Yoshiyuki; Yoshida, Atsusi; Furuta, Takumi; Wakimoto, Toshiyuki; Akizawa, Toshifumi; Konishi, Motomi; Kan, Toshiyuki
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 15 p. 4171 - 4174
反应条件
1: oxalyl chloride; DMF / CH2Cl2 / 3 h / Heating
2: DMAP / CH2Cl2 / 20 °C
3: 83 percent / H2 / Pd(OH)2/C / tetrahydrofuran; methanol / 6 h / 20 °C
View Scheme
参考文献
Wan, Sheng Biao; Ping Dou; Chan, Tak Hang
Tetrahedron, 2006 , vol. 62, # 25 p. 5897 - 5904
反应条件
1: DMAP / CH2Cl2 / 20 °C
2: 83 percent / H2 / Pd(OH)2/C / tetrahydrofuran; methanol / 6 h / 20 °C
View Scheme
参考文献
Wan, Sheng Biao; Ping Dou; Chan, Tak Hang
Tetrahedron, 2006 , vol. 62, # 25 p. 5897 - 5904
