5-(3-丁烯-2-基氧基)-1,3-二甲氧基-2-甲基苯合成路线 （共 3 条）
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran
T=60°C;
参考文献
Zhang, Haiming; Ferreira, Eric M.; Stoltz, Brian M.
Angewandte Chemie - International Edition, 2004 , vol. 43, # 45 p. 6144 - 6148
反应条件
1.1: n-BuLi / hexane; tetrahydrofuran / 1 h / 23 °C
1.2: 93 percent / tetrahydrofuran; hexane / 0.5 h
2.1: 100 percent / HCl / ethanol; H2O / 20 h / 23 °C
3.1: 41 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 60 °C
View Scheme
参考文献
Zhang, Haiming; Ferreira, Eric M.; Stoltz, Brian M.
Angewandte Chemie - International Edition, 2004 , vol. 43, # 45 p. 6144 - 6148
反应条件
1: 100 percent / HCl / ethanol; H2O / 20 h / 23 °C
2: 41 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 60 °C
View Scheme
参考文献
Zhang, Haiming; Ferreira, Eric M.; Stoltz, Brian M.
Angewandte Chemie - International Edition, 2004 , vol. 43, # 45 p. 6144 - 6148
