(4Z)-4-(2,4-二氟苄亚基)-2-甲基-1,3-恶唑-5(4H)-酮合成路线 （共 3 条）
反应条件
sodium acetate; acetic anhydride
Erlenmeyer reaction; 1 h; Heating;
参考文献
Marino, Sharon T.; Stachurska-Buczek, Danuta; Huggins, Daniel A.; Krywult, Beata M.; Sheehan, Craig S.; Nguyen, Thao; Choi, Neil; Parsons, Jack G.; Griffiths, Peter G.; James, Ian W.; Bray, Andrew M.; White, Jonathan M.; Boyce, Rustum S.
Molecules, 2004 , vol. 9, # 6 p. 405 - 426
反应条件
in water; acetone
4 h; Heating;
参考文献
Marino, Sharon T.; Stachurska-Buczek, Danuta; Huggins, Daniel A.; Krywult, Beata M.; Sheehan, Craig S.; Nguyen, Thao; Choi, Neil; Parsons, Jack G.; Griffiths, Peter G.; James, Ian W.; Bray, Andrew M.; White, Jonathan M.; Boyce, Rustum S.
Molecules, 2004 , vol. 9, # 6 p. 405 - 426
反应条件
1: 75.6 percent / acetone; H2O / 4 h / Heating
2: (+)-[(COD)Rh(S,S)-DuPHOS)]-BF4; H2 / methanol / 20 °C / 1551.44 Torr
3: SOCl2 / Heating
4: LiAlH4 / tetrahydrofuran / 1 h / 20 °C
View Scheme
参考文献
Marino, Sharon T.; Stachurska-Buczek, Danuta; Huggins, Daniel A.; Krywult, Beata M.; Sheehan, Craig S.; Nguyen, Thao; Choi, Neil; Parsons, Jack G.; Griffiths, Peter G.; James, Ian W.; Bray, Andrew M.; White, Jonathan M.; Boyce, Rustum S.
Molecules, 2004 , vol. 9, # 6 p. 405 - 426
