hydrogen; palladium on activated charcoal in methanol; ethyl acetate
T=20°C; P=2585.74 Torr; 8 h;
参考文献
Tangallapally, Rajendra P.; Yendapally, Raghunandan; Lee, Robin E.; Lenaerts, Anne J. M.; Lee, Richard E.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 26 p. 8261 - 8269
1: 95 percent / K2CO3 / dimethylsulfoxide / 8 h / 90 °C
2: 100 percent / H2 / Pd/C / ethyl acetate; methanol / 8 h / 20 °C / 2585.74 Torr
View Scheme
参考文献
Tangallapally, Rajendra P.; Yendapally, Raghunandan; Lee, Robin E.; Lenaerts, Anne J. M.; Lee, Richard E.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 26 p. 8261 - 8269
1: 95 percent / K2CO3 / dimethylsulfoxide / 8 h / 90 °C
2: 100 percent / H2 / Pd/C / ethyl acetate; methanol / 8 h / 20 °C / 2585.74 Torr
View Scheme
参考文献
Tangallapally, Rajendra P.; Yendapally, Raghunandan; Lee, Robin E.; Lenaerts, Anne J. M.; Lee, Richard E.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 26 p. 8261 - 8269