1,1,1-三氯-4-乙氧基-3-丁烯-2-酮合成路线 （共 9 条）
反应条件
acetic acid in ethanol T=80°C;
参考文献
Bonacorso, Helio Gauze; Bittencourt, Sandra R. T.; Wastowski, Arci D.; Wentz, Alexandre P.; Zanatta, Nilo; Martins, Marcos A. P.
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 1 p. 45 - 48
反应条件
triethylamine in toluene 0.5 h; Heating;
参考文献
Zanatta, Nilo; Amaral, Simone S.; Esteves-Souza, Andressa; Echevarria, Aurea; Brondani, Patricia B.; Flores, Darlene C.; Bonacorso, Helio G.; Flores, Alex F. C.; Martins, Marcos A. P.
Synthesis, 2006 , # 14 p. 2305 - 2312
反应条件
triethylamine in toluene 2 h; Heating;
参考文献
Zanatta, Nilo; Amaral, Simone S.; Esteves-Souza, Andressa; Echevarria, Aurea; Brondani, Patricia B.; Flores, Darlene C.; Bonacorso, Helio G.; Flores, Alex F. C.; Martins, Marcos A. P.
Synthesis, 2006 , # 14 p. 2305 - 2312
反应条件
pyridine; hydroxylamine hydrochloride in water 24 h; Ambient temperature; Yield given;
参考文献
Spiegler; Gotz
Synthesis, 1986 , vol. NO. 1, p. 69 - 70
反应条件
17 h; Ambient temperature;
参考文献
Gao, Mingzhang; Wang, Min; Zheng, Qi-Huang
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 1 p. 254 - 257
参考文献
Effenberger, Franz; Maier, Roland; Schoenwaelder, Karl-Heinz; Ziegler, Thomas
Chemische Berichte, 1982 , vol. 115, p. 2766 - 2782
反应条件
triethylamine
1) 0 deg C, 17 h, 2) 0 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Effenberger, Franz; Maier, Roland; Schoenwaelder, Karl-Heinz; Ziegler, Thomas
Chemische Berichte, 1982 , vol. 115, p. 2766 - 2782
反应条件
in diethyl ether
T=0°C; 2 h;
参考文献
Effenberger, Franz; Maier, Roland; Schoenwaelder, Karl-Heinz; Ziegler, Thomas
Chemische Berichte, 1982 , vol. 115, p. 2766 - 2782
反应条件
sodium hydroxide in water
T=50°C; 5 h;
参考文献
Zanatta, Nilo; Madruga, Claudia C.; Marisco, Patricia C.; Da Rosa, Luciana S.; Da Silva, Fabio M.; Bonacorso, Helio G.; Martins, Marcos A. P.
Journal of Heterocyclic Chemistry, 2010 , vol. 47, # 5 p. 1234 - 1239
