2,3,4,5,6-五氟苯磺酰氯合成路线 （共 32 条）
反应条件
1: 90.1 percent / tetrahydrofuran; diethyl ether / 2 h / Ambient temperature 2: 17.6 percent / NaI (8), p-DNB / bis-(2-methoxy-ethyl) ether / 10 h / 80 °C / other or none additive; electron transfer reaction of other polyfluorophenyl pentafluorobenzenesulphonates View Scheme
参考文献
Chen, Qing-Yun; Chen, Ming-Fang
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 7 p. 1071 - 1075
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
反应条件
copper
T=200°C; 80 h;
参考文献
Bogachev, A. A.; Kobrina, L. S.; Yakobson, G. G.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 5 p. 967 - 975
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 5 p. 1063 - 1073
反应条件
in diethyl ether
the mixt. in diethyl ether was stirred overnight (N2); the solvent was removed in vac., the residue was dissolved in CH2Cl2, chromy. on silica gel column with CH2Cl2, recrystd. from CH2Cl2-hexane; elem. anal.;
参考文献
El-Khateeb, Mohammad; Shaver, Alan; Lebuis, Anne-Marie
Journal of Organometallic Chemistry, 2001 , vol. 622, # 1-2 p. 293 - 296
反应条件
in tetrahydrofuran
N2-atmosphere; stirring of equimolar amts. (<=30°C, 19 h); solvent removal, chromy. (Al2O3 or Florisil); elem. anal.;
参考文献
Downs, R. L.; Wojcicki, A.
Inorganica Chimica Acta, 1978 , vol. 27, p. 91 - 104
反应条件
copper
T=200°C; 80 h;
参考文献
Bogachev, A. A.; Kobrina, L. S.; Yakobson, G. G.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 5 p. 967 - 975
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 5 p. 1063 - 1073
反应条件
T=570 - 610°C; co-pyrolysis; 1 h;
参考文献
Platonov; Osina; Maksimov; Kolechkina
Journal of Fluorine Chemistry, 1999 , vol. 96, # 2 p. 191 - 192
反应条件
triethylamine in diethyl ether
T=0°C;
参考文献
Shealy, Y. Fulmer; Krauth, Charles A.; Struck, Robert F.; Montgomery, John A.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 8 p. 1168 - 1173
