2′,4′,6′-三甲氧基苯乙酮合成路线 （共 68 条）
反应条件
1: phloroglucinol trimethyl ether in dichloromethane T=0°C; 0.166667 h; 2: acetyl chloride With AlCl3, aluminium chloride in dichloromethane Friedel-Crafts Acylation; 2 h;
参考文献
Zhang, Wen-Jing; Wu, Jing-Fang; Zhou, Peng-Fei; Wang, Yang; Hou, Ai-Jun
Tetrahedron, 2013 , vol. 69, # 29 p. 5850 - 5858
反应条件
scandium tris(trifluoromethanesulfonate) in acetonitrile Friedel-Crafts Acylation; 0.5 h; Inert atmosphereMicrowave irradiationHeatingGreen chemistry; Time;
参考文献
Perrier, Arnaud; Keller, Michel; Caminade, Anne-Marie; Majoral, Jean-Pierre; Ouali, Armelle
Green Chemistry, 2013 , vol. 15, # 8 p. 2075 - 2080
反应条件
sodium hydroxide in acetone 24 h; Reflux;
参考文献
Bello, Murilo Lamim; Chiaradia, Louise Domeneghini; Dias, Luiza Rosaria Sousa; Pacheco, Leticia Kramer; Stumpf, Taisa Regina; Mascarello, Alessandra; Steindel, Mario; Yunes, Rosendo Augusto; Castro, Helena Carla; Nunes, Ricardo Jose; Rodrigues, Carlos Rangel
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 16 p. 5046 - 5052
反应条件
1: With hydrogenchloride; zinc(II) chloride in diethyl ether T=0 - 5°C; 72 h; 2: With water in diethyl ether T=60°C; 2 h;
参考文献
Sagrera, Gabriel; Seoane, Gustavo
Synthesis, 2010 , # 16 art. no. M06509SS, p. 2776 - 2786
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide in sodium hydroxide; chloroform Ambient temperature;
参考文献
Nath, Swadhin; Bhattacharyya, Anjan; Sengupta, P. K.
Journal of the Indian Chemical Society, 1983 , vol. 60, p. 801 - 802
反应条件
1: With palladium (II) trifluoroacetate; 6-mbipy in water T=130°C; 1 h; Microwave irradiation; 2: With formic acid in water T=100°C; 1 h;
参考文献
Lindh, Jonas; Sjoeberg, Per J. R.; Larhed, Mats
Angewandte Chemie - International Edition, 2010 , vol. 49, # 42 p. 7733 - 7737
反应条件
sodium perchlorate; acetic acid T=70°C;
参考文献
Journal of the American Chemical Society, , vol. 79, p. 3582,3585
反应条件
1: 1.) AlCl3; 2.) H2O, conc HCl / 1.) Et2O, reflux, 1 h then r.t., overnight 2: diethyl ether View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 28, # 11 p. 3193 - 3196
反应条件
1: folgende Methylierung mit Dimethylsulfat und Kalilauge 2: iron chloride View Scheme
参考文献
Chemische Berichte, , vol. 53, p. 1427
Chemische Berichte, , vol. 55, p. 1941
反应条件
1: potassium carbonate / acetone 2: sodium hydroxide / acetone / 24 h / Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 19, # 16 p. 5046 - 5052
