2′,4′,6′-三甲氧基苯乙酮合成路线 （共 68 条）
反应条件
aluminium trichloride in chlorobenzene 1 h; Heating;
参考文献
Asolkar, Ratnakar N.; Kamat, Vijayendra P.; Kirtany, Janardan K.
Journal of Chemical Research - Part S, 2001 , # 12 p. 549 - 550
反应条件
aluminium trichloride in chlorobenzene
参考文献
Malterud, Karl Egil; Undheim, Jorunn; Erdal, John Erik
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4807 - 4810
参考文献
Rennie; Cooke; Finlayson
Journal of the Chemical Society, 1920 , vol. 117, p. 348
反应条件
trifluoromethylsulfonic anhydride; NMe4NO3 in dichloromethane T=-78 - 20°C; 50 h;
参考文献
Shackelford, Scott A.; Anderson, Mark B.; Christie, Lance C.; Goetzen, Thomas; Guzman, Mark C.; Hananel, Martha A.; Kornreich, Wayne D.; Li, Haitao; Pathak, Ved P.; Rabinovich, Alex K.; Rajapakse, Ranjan J.; Truesdale, Larry K.; Tsank, Stella M.; Vazir, Haresh N.
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 267 - 275
反应条件
nitric acid in acetic anhydride; acetic acid 12 h;
参考文献
Acton, John P.; Donnelly, Dorothy J.; Donnelly, John A.
Monatshefte fuer Chemie, 1982 , vol. 113, p. 73 - 80
反应条件
1: 99 percent / KOH / ethanol / 3 h / 20 °C 2: 90 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C 3: 93 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.33 h / 0 - 20 °C 4: 41 percent / K2CO3 / acetone / 1 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 60, # 11 p. 2647 - 2655
反应条件
1: AcOOH, HClO4, Ac2O 2: KOH / ethanol / Heating View Scheme
参考文献
Huee,R. et al.
Bulletin de la Societe Chimique de France, 1970 , p. 3617 - 3624
反应条件
1.1: boron trichloride / dichloromethane / 2 h / 0 °C 1.2: 1 h 2.1: potassium hydroxide / methanol / 80 h / 20 °C 2.2: pH 5 - 6 3.1: iodine / dimethyl sulfoxide / 4 h / 120 °C View Scheme
参考文献
Liu, Man; Zhang, Ji; Yang, Jian; Yang, Bo; Cui, Wei
Journal of Chemical Research, 2014 , vol. 38, # 3 p. 134 - 136
反应条件
1: 99 percent / KOH / ethanol / 3 h / 20 °C 2: 90 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C 3: 65 percent / dimethyl dioxirane / acetone; CH2Cl2 / 1 h / 0 - 20 °C 4: 95 percent / K2CO3 / acetone / 6 h / Heating 5: 71 percent / I2; pyridine / 8 h / Heating View Scheme
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
反应条件
1: 99 percent / KOH / ethanol / 3 h / 20 °C 2: 90 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C 3: 97 percent / K2CO3 / acetone / 2 h / Heating 4: 86 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.5 h / 0 - 20 °C 5: 96 percent / K2CO3 / acetone / 1 h / Heating 6: 99 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 11 p. 2647 - 2655
