Jackson, Anthony H.; Shannon, Patrick V. R.; Taylor, Paul W.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 286 - 297
1: 93 percent / lithium aluminium hydride / tetrahydrofuran / 2 h / Heating
2: 81 percent / pyridine, thionyl chloride / 2 h / Heating
3: 75 percent / dimethylsulfoxide / 2.5 h / 80 °C
4: 1.65 g / potassium hydroxyde / H2O; various solvent(s) / 10 h / Heating
5: 960 mg / lithium aluminium hydride / tetrahydrofuran / 3 h / Heating
6: 1.) boron trifluoride-ether; 2.) dichlorodicyanobenzoquinone / 1.) reflux, 4.5 h; 2.) benzene, reflux, 3 h
View Scheme
参考文献
Jackson, Anthony H.; Shannon, Patrick V. R.; Taylor, Paul W.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 286 - 297
1: 75 percent / dimethylsulfoxide / 2.5 h / 80 °C
2: 1.65 g / potassium hydroxyde / H2O; various solvent(s) / 10 h / Heating
3: 960 mg / lithium aluminium hydride / tetrahydrofuran / 3 h / Heating
4: 1.) boron trifluoride-ether; 2.) dichlorodicyanobenzoquinone / 1.) reflux, 4.5 h; 2.) benzene, reflux, 3 h
View Scheme
参考文献
Jackson, Anthony H.; Shannon, Patrick V. R.; Taylor, Paul W.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 286 - 297
1: 1.65 g / potassium hydroxyde / H2O; various solvent(s) / 10 h / Heating
2: 960 mg / lithium aluminium hydride / tetrahydrofuran / 3 h / Heating
3: 1.) boron trifluoride-ether; 2.) dichlorodicyanobenzoquinone / 1.) reflux, 4.5 h; 2.) benzene, reflux, 3 h
View Scheme
参考文献
Jackson, Anthony H.; Shannon, Patrick V. R.; Taylor, Paul W.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 286 - 297
1: 81 percent / pyridine, thionyl chloride / 2 h / Heating
2: 75 percent / dimethylsulfoxide / 2.5 h / 80 °C
3: 1.65 g / potassium hydroxyde / H2O; various solvent(s) / 10 h / Heating
4: 960 mg / lithium aluminium hydride / tetrahydrofuran / 3 h / Heating
5: 1.) boron trifluoride-ether; 2.) dichlorodicyanobenzoquinone / 1.) reflux, 4.5 h; 2.) benzene, reflux, 3 h
View Scheme
参考文献
Jackson, Anthony H.; Shannon, Patrick V. R.; Taylor, Paul W.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 286 - 297
