反应条件
1: sodium periodate / tetrahydrofuran; H2O / 4 h / Ambient temperature
2: 25 percent / n-BuLi / diethyl ether; hexane / 1.) -78 deg C, 8 h; -50 deg C, 4 h, 2.) t-butyl alcohol, room temp., overnight
3: 91 percent / NaOH / ethanol / Ambient temperature
4: 80 percent / diethyl ether / Ambient temperature
View Scheme
参考文献
Takaiwa, Akihiro; Yamashita, Kyohei
Agricultural and Biological Chemistry, 1984 , vol. 48, # 8 p. 2061 - 2066
