反应条件
1: 1,8-dichloro-9,10-ethano-9,10-dihydroanthracene With sodium; lithium in tetrahydrofuran
T=-78°C; 6 h; Inert atmosphere;
2: chloro-diphenylphosphine in tetrahydrofuran
T=-78 - 20°C; Inert atmosphere;
参考文献
Tauchert, Michael E.; Warth, Daniel C. M.; Braun, Sebastian M.; Gruber, Irene; Ziesak, Alexandra; Rominger, Frank; Hofmann, Peter
Organometallics, 2011 , vol. 30, # 10 p. 2790 - 2809