1: 48 percent / o-chloranil / dioxane / Heating; overnight
2: 83 percent / 1 N NaOMe / tetrahydrofuran; methanol / 1 h / -20 °C
3: 66 percent / 99percent m-chloroperoxybenzoic acid / CHCl3 / 1 h / 0 °C
View Scheme
参考文献
Rastetter, William H.; Nachbar, Robert B.; Russo-Rodriguez, Sandra; Wattley, Ruth V.; Thilly, William G.; et al.
Journal of Organic Chemistry, 1982 , vol. 47, # 25 p. 4873 - 4878