10,11-二氢-5H-二苯并[a,d]环庚烯合成路线 （共 47 条）
反应条件
(i) Na-K, Et2O, (ii) CO2, aq. EtOH; Multistep reaction;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 84, p. 1466 - 1477
反应条件
(i) KOtBu, tBuOH, (ii) H2O; Multistep reaction;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 718, p. 33 - 49
反应条件
trimethylsilylazide; diphenyl phosphoryl azide; water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride in acetic acid; trifluoroacetic acid T=80°C; 48 h; Inert atmosphere;
参考文献
Qin, Chong; Zhou, Wang; Chen, Feng; Ou, Yang; Jiao, Ning
Angewandte Chemie - International Edition, 2011 , vol. 50, # 52 p. 12595 - 12599
反应条件
2-iodo benzoic acid; potassium hydrogen persulfate; water in acetonitrile
参考文献
Ojha, Lawanya R.; Kudugunti, Shashi; Maddukuri, Padma P.; Kommareddy, Amitha; Gunna, Meena R.; Dokuparthi, Praveen; Gottam, Hima B.; Botha, Kiran K.; Parapati, Divya R.; Vinod, Thottumkara K.
Synlett, 2009 , # 1 p. 117 - 121
反应条件
aluminum oxide; Ru(OH)x; oxygen in 1,2-dichloro-benzene T=169.85°C; P=760 Torr; 5 h;
参考文献
Kamata, Keigo; Kasai, Jun; Yamaguchi, Kazuya; Mizuno, Noritaka
Organic Letters, 2004 , vol. 6, # 20 p. 3577 - 3580
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile; sodium hydrogensulfite 1.) benzene, irrad., 22 h, 2.) benzene; Yield given. Multistep reaction;
参考文献
Mataka, Shuntaro; Liu, Guo-Bin; Tori-I, Akiyoshi; Tashiro, Masashi
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 8 p. 2336 - 2338
反应条件
aluminum oxide; Ru(OH)x; oxygen in 1,2-dichloro-benzene T=169.85°C; P=760 Torr; 5 h;
参考文献
Kamata, Keigo; Kasai, Jun; Yamaguchi, Kazuya; Mizuno, Noritaka
Organic Letters, 2004 , vol. 6, # 20 p. 3577 - 3580
