Colletochlorin B合成路线 （共 12 条）
反应条件
1.1: hydrogenchloride / diethyl ether / 2 h / |Inert atmosphere
1.2: 100 °C
2.1: sulfuryl dichloride / diethyl ether / |Inert atmosphere; |Cooling with ice
3.1: potassium hydroxide / |Cooling with ice
View Scheme
参考文献
THE UNIVERSITY OF SUSSEX; MOORE, Anthony Lennox; ALBURY, Mary Susan; YOUNG, Luke Edward; ELLIOTT, Catherine
Patent: WO2013/160670 A1, 2013 ;
反应条件
water; acetic acid
1) 110-120 deg C, 3 h, 2) reflux, 3 h; Yield given. Multistep reaction;
参考文献
Mori, Kenji; Sato, Kazuo
Tetrahedron, 1982 , vol. 38, # 9 p. 1221 - 1225
