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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
83326-76-5
合成路线
（共 10 条）
1357171-06-2
→
反应条件
83326-76-5
反应条件
1: With potassium hydroxide in tetrahydrofuran; water T=55°C; 2: With hydrogenchloride in tetrahydrofuran; water; ethyl acetate
参考文献
Ghizzoni, Massimo; Wu, Jiang; Gao, Tielong; Haisma, Hidde J.; Dekker, Frank J.; George Zheng
European Journal of Medicinal Chemistry, 2012 , vol. 47, # 1 p. 337 - 344
86791-43-7
→
反应条件
83326-76-5
反应条件
potassium hydroxide in water; dimethyl sulfoxide T=90°C; 20 h;
参考文献
Shibuya; Ebizuka; Noguchi; Iitaka; Sankawa
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 407 - 413
591-31-1
3-甲氧基苯甲醛
→
反应条件
83326-76-5
反应条件
1: 55 percent / 2.) dil. HCl / hexane / -78 °C 2: 68 percent / AlCl3 / 6 h / 120 °C 3: 1.) KOH / 2.) Raney Ni (W-2) / 1.) H2O, reflux, 80 min, 2.) RT, 2 h, EtOH View Scheme
参考文献
Nishikawa, Asuka; Hashimoto, Yuichi; Shirai, Ryuichi
Tetrahedron Letters, 1998 , vol. 39, # 40 p. 7307 - 7308
38862-65-6
→
反应条件
83326-76-5
反应条件
1: 3.2 g / K2CO3 / acetone / 15 h / Heating 2: AcONa, H2 / Pd-C (10percent) / acetic acid / Ambient temperature 3: 80 percent / KOH / H2O; dimethylsulfoxide / 20 h / 90 °C View Scheme
参考文献
Shibuya; Ebizuka; Noguchi; Iitaka; Sankawa
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 407 - 413
58497-40-8
→
反应条件
83326-76-5
反应条件
1: 92 percent / AcONa, H2 / Pd-C (10percent) / acetic acid / Ambient temperature 2: 3.2 g / K2CO3 / acetone / 15 h / Heating 3: AcONa, H2 / Pd-C (10percent) / acetic acid / Ambient temperature 4: 80 percent / KOH / H2O; dimethylsulfoxide / 20 h / 90 °C View Scheme
参考文献
Shibuya; Ebizuka; Noguchi; Iitaka; Sankawa
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 407 - 413
86791-42-6
→
反应条件
83326-76-5
反应条件
1: AcONa, H2 / Pd-C (10percent) / acetic acid / Ambient temperature 2: 80 percent / KOH / H2O; dimethylsulfoxide / 20 h / 90 °C View Scheme
参考文献
Shibuya; Ebizuka; Noguchi; Iitaka; Sankawa
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 407 - 413
214750-30-8
→
反应条件
83326-76-5
反应条件
1: 68 percent / AlCl3 / 6 h / 120 °C 2: 1.) KOH / 2.) Raney Ni (W-2) / 1.) H2O, reflux, 80 min, 2.) RT, 2 h, EtOH View Scheme
参考文献
Nishikawa, Asuka; Hashimoto, Yuichi; Shirai, Ryuichi
Tetrahedron Letters, 1998 , vol. 39, # 40 p. 7307 - 7308
164014-48-6
→
反应条件
83326-76-5
反应条件
1: palladium 10 on activated carbon; hydrogen / methanol / 40 °C / 2280.15 Torr / Autoclave 2: potassium hydroxide / tetrahydrofuran; water / 55 °C View Scheme
参考文献
Ghizzoni, Massimo; Wu, Jiang; Gao, Tielong; Haisma, Hidde J.; Dekker, Frank J.; George Zheng
European Journal of Medicinal Chemistry, 2012 , vol. 47, # 1 p. 337 - 344
627-19-0
1-戊炔
→
反应条件
83326-76-5
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diethylamine / acetonitrile / 0.5 h / 100 °C / Inert atmosphere; Microwave irradiation 2: palladium 10 on activated carbon; hydrogen / methanol / 40 °C / 2280.15 Torr / Autoclave 3: potassium hydroxide / tetrahydrofuran; water / 55 °C View Scheme
参考文献
Ghizzoni, Massimo; Wu, Jiang; Gao, Tielong; Haisma, Hidde J.; Dekker, Frank J.; George Zheng
European Journal of Medicinal Chemistry, 2012 , vol. 47, # 1 p. 337 - 344
164014-40-8
→
反应条件
83326-76-5
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diethylamine / acetonitrile / 0.5 h / 100 °C / Inert atmosphere; Microwave irradiation 2: palladium 10 on activated carbon; hydrogen / methanol / 40 °C / 2280.15 Torr / Autoclave 3: potassium hydroxide / tetrahydrofuran; water / 55 °C View Scheme
参考文献
Ghizzoni, Massimo; Wu, Jiang; Gao, Tielong; Haisma, Hidde J.; Dekker, Frank J.; George Zheng
European Journal of Medicinal Chemistry, 2012 , vol. 47, # 1 p. 337 - 344
