6-(羟基甲基)-6H-二苯并[b,d]吡喃-6-甲腈合成路线 （共 3 条）
反应条件
sodium methylate in dimethyl sulfoxide
T=20 - 25°C; 5 h;
参考文献
Banzatti; Branzoli; Lovisolo; Melloni; Orsini; Salvadori
Arzneimittel-Forschung/Drug Research, 1984 , vol. 34, # 8 p. 864 - 869
反应条件
1: 83 percent / 1.2M diisobutyl aluminium hydride / toluene / 1 h / -70 °C
2: 90 percent / ZnI2 / benzene / 0.5 h / Ambient temperature
3: 91 percent / sodium methylate / dimethylsulfoxide / 5 h / 20 - 25 °C
View Scheme
参考文献
Banzatti; Branzoli; Lovisolo; Melloni; Orsini; Salvadori
Arzneimittel-Forschung/Drug Research, 1984 , vol. 34, # 8 p. 864 - 869
反应条件
1: 90 percent / ZnI2 / benzene / 0.5 h / Ambient temperature
2: 91 percent / sodium methylate / dimethylsulfoxide / 5 h / 20 - 25 °C
View Scheme
参考文献
Banzatti; Branzoli; Lovisolo; Melloni; Orsini; Salvadori
Arzneimittel-Forschung/Drug Research, 1984 , vol. 34, # 8 p. 864 - 869
