(9ci)-1H-咪唑-1-羧酸-2-丙烯酯合成路线 (共 6 条)
反应条件
sec-phenethyl alcohol; sodium hydride in tetrahydrofuran T=0°C; Acylation; 0.5 h;
参考文献
Bertolini, Giorgio; Pavich, Gianfranco; Vergani, Barbara
Journal of Organic Chemistry, 1998 , vol. 63, # 17 p. 6031 - 6034
反应条件
in acetonitrile T=80°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Heller, Stephen T.; Sarpong, Richmond
Tetrahedron, 2011 , vol. 67, # 46 p. 8851 - 8859
反应条件
in acetonitrile-D3 T=80°C; 16 h; Inert atmosphereSealed vial;
参考文献
Tetrahedron, , vol. 67, # 46 p. 8851 - 8859
反应条件
in tetrahydrofuran; dichloromethane
T=0°C; 2 h;
参考文献
Trost, Barry M.; Xu, Jiayi
Journal of Organic Chemistry, 2007 , vol. 72, # 24 p. 9372 - 9375
反应条件
in tetrahydrofuran
T=0 - 20°C; 5 h; Inert atmosphere;
参考文献
Heller, Stephen T.; Sarpong, Richmond
Organic Letters, 2010 , vol. 12, # 20 p. 4572 - 4575
反应条件
in N,N-dimethyl-formamide
T=80°C; 24 h; Inert atmosphereSealed vial;
参考文献
Heller, Stephen T.; Sarpong, Richmond
Tetrahedron, 2011 , vol. 67, # 46 p. 8851 - 8859