4 -甲氧基二苯基甲烷合成路线 (共 196 条)
反应条件
iron tribromide in 1,2-dichloro-ethane
T=80°C; Friedel Crafts alkylation; 24 h; Air; regioselective reaction;
参考文献
Guo, Xiao-Kang; Zhao, Dong-Yun; Li, Jin-Heng; Zhang, Xing-Guo; Deng, Chen-Liang; Tang, Ri-Yuan
Synlett, 2012 , # 4 p. 627 - 631
反应条件
titanium
T=110 - 140°C;
参考文献
Sharma; Dutt
Journal of the Indian Chemical Society, 1935 , vol. 12, p. 774,776
反应条件
digallium tetrachloride in benzene
Ambient temperature;
参考文献
Hashimoto; Hirata; Kihara; Hasegawa; Saigo
Tetrahedron Letters, 1992 , vol. 33, # 42 p. 6351 - 6354
反应条件
indium trifluoromethanesulfonate; 1-ethyl-3-methylimidazolium bistrifluoromethylsulfonylamide
T=120°C; Friedel-Crafts Alkylation; 1.5 h; Microwave irradiationGreen chemistry;
参考文献
Mack, Ryan; Askins, Grant; Lowry, Jacob; Hurley, Nathan; Reeves, Perry C.
Canadian Journal of Chemistry, 2013 , vol. 91, # 12 p. 1262 - 1265
反应条件
trifluorormethanesulfonic acid
T=100°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Fukuzawa, Shin-Ichi; Tsuchimoto, Teruhisa; Hiyama, Tamejiro
Journal of Organic Chemistry, 1997 , vol. 62, # 1 p. 151 - 156
反应条件
scandium tris(trifluoromethanesulfonate) in nitromethane
1 h; Heating; Yield given. Yields of byproduct given;
参考文献
Tsuchimoto, Teruhisa; Tobita, Kazuo; Hiyama, Tamejiro; Fukuzawa, Shin-Ichi
Journal of Organic Chemistry, 1997 , vol. 62, # 20 p. 6997 - 7005
反应条件
indium tribromide
T=60°C; 1 h; Inert atmosphere;
参考文献
Sakai, Norio; Kawana, Keita; Ikeda, Reiko; Nakaike, Yumi; Konakahara, Takeo
European Journal of Organic Chemistry, 2011 , # 17 p. 3178 - 3183
反应条件
indium tribromide; phenyl silane
T=60°C; 1 h; Inert atmosphere;
参考文献
Sakai, Norio; Kawana, Keita; Ikeda, Reiko; Nakaike, Yumi; Konakahara, Takeo
European Journal of Organic Chemistry, 2011 , # 17 p. 3178 - 3183
反应条件
in tetrahydrofuran
T=70°C; 8 h;
参考文献
Li, Man-Bo; Tang, Xiang-Ling; Tian, Shi-Kai
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1980 - 1984
反应条件
potassium cyanide; aluminum oxide
T=50°C; 48 h;
参考文献
Ando, Takashi; Sumi, Shinjiro; Kawate, Takehiko; Ichihara, Junko; Hanafusa, Terukiyo
Journal of the Chemical Society, Chemical Communications, 1984 , # 7 p. 439 - 440