4 -甲氧基二苯基甲烷合成路线 （共 196 条）
反应条件
palladium on carbon; hydrogen in methanol
T=20°C; 16 h;
参考文献
Cheng, Ying; Dong, Wanrong; Wang, Long; Parthasarathy, Kanniyappan; Bolm, Carsten
Organic Letters, 2014 , vol. 16, # 7 p. 2000 - 2002
反应条件
palladium diacetate; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=40°C; 1 h; Inert atmosphere;
参考文献
Chang, Shu-Ting; Li, Qinghan; Chiang, Ruei-Tang; Gau, Han-Mou
Tetrahedron, 2012 , vol. 68, # 21 p. 3956 - 3962
反应条件
tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; lithium chloride in N,N-dimethyl-formamide
T=20°C; Stille Cross Coupling; 12 h; SonicationInert atmosphere;
参考文献
Ocampo, Romina A.; Koll, Liliana C.; Mandolesi, Sandra D.
Ultrasonics Sonochemistry, 2013 , vol. 20, # 1 p. 40 - 46
反应条件
1,5-bis-(diphenylphosphino)-pentane; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide
T=80°C; Suzuki-Miyaura reaction; 24 h;
参考文献
Kuwano, Ryoichi; Yokogi, Masashi
Organic Letters, 2005 , vol. 7, # 5 p. 945 - 947
反应条件
1,5-bis-(diphenylphosphino)-pentane; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide
T=80°C; Suzuki-Miyaura reaction; 5 h;
参考文献
Kuwano, Ryoichi; Yokogi, Masashi
Organic Letters, 2005 , vol. 7, # 5 p. 945 - 947
反应条件
potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether; bis(η3-allyl-μ-chloropalladium(II)) in 1,1-dimethylpropan-1-ol
T=80°C; 3 h;
参考文献
Kuwano, Ryoichi; Yokogi, Masashi
Chemical Communications, 2005 , # 47 p. 5899 - 5901
反应条件
1: benzyl bromide With zinc in tetrahydrofuran
T=0°C; 2 h;
2: 4-methoxyphenyl triflate With 1,1'-bis-(diphenylphosphino)ferrocene; tetra-(n-butyl)ammonium iodide; bis(dibenzylideneacetone) palladium in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=60°C; 6 h; Further stages.;
参考文献
Piber, Michael; Jensen, Anne Eeg; Rottlaender, Mario; Knochel, Paul
Organic Letters, 1999 , vol. 1, # 9 p. 1323 - 1326
反应条件
tetrakis(triphenylphosphine) palladium(0); silver(l) oxide in tetrahydrofuran
T=60°C; Arylation; 36 h;
参考文献
Hirabayashi, Kazunori; Kawashima, Jun; Nishihara, Yasushi; Mori, Atsunori; Hiyama, Tamejiro
Organic Letters, 1999 , vol. 1, # 2 p. 299 - 301
反应条件
N,N,N',N,-tetramethylethylenediamine; mono(bis(di-tert-butyl(4-(dimethylamino)phenyl)phosphonio)palladium(II))dichloride; zinc in water
T=20°C; 8 h; Inert atmosphere;
参考文献
Duplais, Christophe; Krasovskiy, Arkady; Wattenberg, Alina; Lipshutz, Bruce H.
Chemical Communications, 2010 , vol. 46, # 4 p. 562 - 564
反应条件
caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran; water
T=77°C; Suzuki-Miyaura cross-coupling; 18 h;
参考文献
Molander, Gary A.; Elia, Maxwell D.
Journal of Organic Chemistry, 2006 , vol. 71, # 24 p. 9198 - 9202
