4 -甲氧基二苯基甲烷合成路线 (共 196 条)
反应条件
caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran; water
T=77°C; Suzuki-Miyaura cross-coupling; 20 h;
参考文献
Molander, Gary A.; Elia, Maxwell D.
Journal of Organic Chemistry, 2006 , vol. 71, # 24 p. 9198 - 9202
反应条件
caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran; water
T=77°C; Suzuki-Miyaura cross-coupling;
参考文献
Molander, Gary A.; Elia, Maxwell D.
Journal of Organic Chemistry, 2006 , vol. 71, # 24 p. 9198 - 9202
反应条件
caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in water
T=90°C; Suzuki-Miyaura cross-coupling; 14 h;
参考文献
Molander, Gary A.; Elia, Maxwell D.
Journal of Organic Chemistry, 2006 , vol. 71, # 24 p. 9198 - 9202
反应条件
N,N,N',N,-tetramethylethylenediamine; mono(bis(di-tert-butyl(4-(dimethylamino)phenyl)phosphonio)palladium(II))dichloride; zinc in water
T=20°C; 8 h; Inert atmosphere;
参考文献
Duplais, Christophe; Krasovskiy, Arkady; Wattenberg, Alina; Lipshutz, Bruce H.
Chemical Communications, 2010 , vol. 46, # 4 p. 562 - 564
反应条件
ethanol; nickel
5 h; Heating;
参考文献
Khim, Seock-Kyu; Dai, Mingshi; Zhang, Xuqing; Chen, Lei; Pettus, Liping; Thakkar, Kshitij; Schultz, Arthur G.
Journal of Organic Chemistry, 2004 , vol. 69, # 22 p. 7728 - 7733
反应条件
lithium chloride; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; N,N-dimethyl-formamide
T=80°C; Stille coupling; 22 h;
参考文献
Hoshino, Masahide; Degenkolb, Peter; Curran, Dennis P.
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8341 - 8349
反应条件
silver(l) oxide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=60°C;
参考文献
Itami, Kenichiro; Mineno, Masahiro; Kamei, Toshiyuki; Yoshida, Jun-Ichi
Organic Letters, 2002 , vol. 4, # 21 p. 3635 - 3638
反应条件
triethylsilane; bis-(trifluoromethylsulphonyl)amine in dichloromethane
T=20°C; 2 h;
参考文献
Yang, Bai-Ling; Tian, Shi-Kai
Chemical Communications, 2010 , vol. 46, # 33 p. 6180 - 6182
反应条件
FeCl(THF)L1 in diethyl ether; dichloromethane
T=20°C; 0.5 h; Inert atmosphereSchlenk technique;
参考文献
Chard, Elliott F.; Dawe, Louise N.; Kozak, Christopher M.
Journal of Organometallic Chemistry, 2013 , vol. 737, p. 32 - 39
反应条件
palladium diacetate; potassium phosphate; triphenylphosphine in toluene
T=90°C; Suzuki-Miyaura coupling; 16 h;
参考文献
McLaughlin, Mark
Organic Letters, 2005 , vol. 7, # 22 p. 4875 - 4878