4 -甲氧基二苯基甲烷合成路线 （共 196 条）
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium phosphate in tetrahydrofuran; N,N-dimethyl-formamide
T=60°C; Suzuki-Miyaura reaction; 16 h;
参考文献
Flaherty, Alice; Trunkfield, Amy; Barton, William
Organic Letters, 2005 , vol. 7, # 22 p. 4975 - 4978
反应条件
FeCl2(dppbz)2 in tetrahydrofuran; toluene
T=45°C; Negishi coupling; 4 h; Inert atmosphere;
参考文献
Bedford, Robin B.; Huwe, Michael; Wilkinson, Mark C.
Chemical Communications, 2009 , # 5 p. 600 - 602
反应条件
sodium hydroxide; tetrabutylammomium bromide; palladium dichloride in water
T=130 - 160°C; 1 h; Microwave irradiation;
参考文献
Schmink, Jason R.; Leadbeater, Nicholas E.
Organic Letters, 2009 , vol. 11, # 12 p. 2575 - 2578
反应条件
C36H44Cl6O4P2Pd2 in tetrahydrofuran
T=60°C; Kumada-Corriu coupling; 24 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Kapdi, Anant R.; Schulzke, Carola
Organic Letters, 2010 , vol. 12, # 10 p. 2298 - 2301
反应条件
methanol; palladium 10 on activated carbon; hydrogen; potassium carbonate
T=65°C; P=760.051 Torr; 24 h; Catalytic behavior;
参考文献
Zhou, Lei; Liu, Zhenxing; Liu, Yizhou; Zhang, Yan; Wang, Jianbo
Tetrahedron, 2013 , vol. 69, # 30 p. 6083 - 6087
反应条件
ClSO2F (sulfuryl chloride fluoride); SbF5
T=-90°C;
参考文献
Olah, George A.; Olah, Judith A.; Ohyama, Toshiyuki
Journal of the American Chemical Society, 1984 , vol. 106, # 18 p. 5284 - 5290
反应条件
dihydrogen hexachloroplatinate
T=80°C; Friedel-Crafts alkylation; Title compound not separated from byproducts;
参考文献
Mertins, Kristin; Iovel, Irina; Kischel, Jette; Zapf, Alexander; Beller, Matthias
Angewandte Chemie - International Edition, 2005 , vol. 44, # 2 p. 238 - 242
反应条件
palladium diacetate; potassium phosphate; triphenylphosphine in toluene
T=90°C; Suzuki-Miyaura coupling; 16 h;
参考文献
McLaughlin, Mark
Organic Letters, 2005 , vol. 7, # 22 p. 4875 - 4878
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium phosphate in tetrahydrofuran
T=60°C; Suzuki-Miyaura reaction; 1 h;
参考文献
Flaherty, Alice; Trunkfield, Amy; Barton, William
Organic Letters, 2005 , vol. 7, # 22 p. 4975 - 4978
反应条件
methanol; potassium hydroxide
参考文献
Rennie
Journal of the Chemical Society, 1882 , vol. 41, p. 34
