2,2-二甲基-1,3-二氧戊环-4-羧酸钾盐合成路线 （共 6 条）
反应条件
potassium permanganate; potassium hydroxide in water T=0 - 20°C;
参考文献
AUSPEX PHARMACEUTICALS, INC.
Patent: US2009/270469 A1, 2009 ;
Location in patent: Page/Page column 29-30 ;
反应条件
potassium hydroxide; potassium permanganate in water T=20 - 23°C; 1.5 h;
参考文献
Bogoslovskii, N. A.; Samokhvalova, N. G.; Isaeva, T. A.; Valashek, I. E.; Filippova, T. M.; Kharchevnikov, A. P.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 11 p. 2070 - 2081
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 11 p. 2398 - 2411
反应条件
potassium permanganate; sodium periodate Product distribution / selectivity;
参考文献
US2006/30574 A1, ;
Page/Page column 8 ;
反应条件
1: sodium periodate, sodium bicarbonate / H2O / 1 h / 0 - 5 °C 2: 75.3 g / potassium hydroxide, potassium permanganate / H2O / 1.5 h / 20 - 23 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 26, # 11 p. 2070 - 2081
Zhurnal Organicheskoi Khimii, , vol. 26, # 11 p. 2398 - 2411
反应条件
N,N,N',N,-tetramethylethylenediamine in acetonitrile T=60°C; 6 h;
参考文献
AUSPEX PHARMACEUTICALS, INC.
Patent: US2009/270469 A1, 2009 ;
Location in patent: Page/Page column 30 ;
反应条件
in N,N-dimethyl-formamide 3 h;
参考文献
Bogoslovskii, N. A.; Samokhvalova, N. G.; Isaeva, T. A.; Valashek, I. E.; Filippova, T. M.; Kharchevnikov, A. P.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 11 p. 2070 - 2081
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 11 p. 2398 - 2411
