3-(4-(4-氧代-2-(苯基亚胺)-3-噻唑烷基)苯基)-2-(4-((苯基亚甲基)氨基)苯基)-4(3H)-喹唑啉酮合成路线 （共 7 条）
反应条件
1: 70 percent / pyridine / 1 h / 10 °C
2: 65 percent / 0.25 h / Heating
3: 67 percent / N2H4*H2O / Raney nickel / ethanol / 12 h / Heating
4: 62 percent / benzene / 4 h / Heating
5: 52 percent / NaOAc, glacial AcOH / 6 h / Heating
View Scheme
参考文献
Shukla, J. S.; Rastogi, Renu
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 375 - 377
反应条件
1: 65 percent / 0.25 h / Heating
2: 67 percent / N2H4*H2O / Raney nickel / ethanol / 12 h / Heating
3: 62 percent / benzene / 4 h / Heating
4: 52 percent / NaOAc, glacial AcOH / 6 h / Heating
View Scheme
参考文献
Shukla, J. S.; Rastogi, Renu
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 375 - 377
反应条件
1: 67 percent / N2H4*H2O / Raney nickel / ethanol / 12 h / Heating
2: 62 percent / benzene / 4 h / Heating
3: 52 percent / NaOAc, glacial AcOH / 6 h / Heating
View Scheme
参考文献
Shukla, J. S.; Rastogi, Renu
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 375 - 377
反应条件
1: 70 percent / pyridine / 1 h / 10 °C
2: 65 percent / 0.25 h / Heating
3: 67 percent / N2H4*H2O / Raney nickel / ethanol / 12 h / Heating
4: 62 percent / benzene / 4 h / Heating
5: 52 percent / NaOAc, glacial AcOH / 6 h / Heating
View Scheme
参考文献
Shukla, J. S.; Rastogi, Renu
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 375 - 377
反应条件
1: SOCl2
2: 70 percent / pyridine / 1 h / 10 °C
3: 65 percent / 0.25 h / Heating
4: 67 percent / N2H4*H2O / Raney nickel / ethanol / 12 h / Heating
5: 62 percent / benzene / 4 h / Heating
6: 52 percent / NaOAc, glacial AcOH / 6 h / Heating
View Scheme
参考文献
Shukla, J. S.; Rastogi, Renu
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 375 - 377
反应条件
sodium acetate; acetic acid
6 h; Heating;
参考文献
Shukla, J. S.; Rastogi, Renu
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 375 - 377
反应条件
1: 62 percent / benzene / 4 h / Heating
2: 52 percent / NaOAc, glacial AcOH / 6 h / Heating
View Scheme
参考文献
Shukla, J. S.; Rastogi, Renu
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 375 - 377
