4-氨基-5-碘-6-甲基嘧啶合成路线 （共 6 条）
反应条件
ammonia in ethanol T=120°C; 12 h;
参考文献
Sakamoto; Kondo; Yamanaka
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 7 p. 2410 - 2416
反应条件
sulfuric acid; dihydrogen peroxide; iodine in tetrachloromethane; water T=80°C; 1.5 h;
参考文献
Zeuner, F.; Niclas, H.-J.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 2 p. 324 - 330
反应条件
dihydrogen peroxide in water T=100°C; 2 h;
参考文献
Zeuner, F.; Niclas, H.-J.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 2 p. 324 - 330
反应条件
1: 75 percent / POCl3 / 2 h / Heating 2: 80 percent / NH3 / ethanol / 12 h / 120 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 7 p. 2410 - 2416
反应条件
sulfuric acid; water; dihydrogen peroxide; iodine 1.) CCl4, 3 h, 70 deg C, 2.) 1 h, reflux; Yield given. Multistep reaction;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 331, # 2 p. 324 - 330
反应条件
sulfuric acid; dihydrogen peroxide 1.) 1 h, 60 deg C; 1.5 h, 80 deg C, 2.) CCl4, reflux; Yield given. Multistep reaction;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 331, # 2 p. 324 - 330
