甲基2,3,4,6-四-O-苄基-D-吡喃甘露糖苷合成路线 （共 2 条）
反应条件
1: 80percent AcOH, 2 N H2SO4 / H2O / 8 h / 90 °C 2: 1.) NaH / 1.) CH2Cl2, RT, 10 min, 2.) CH2Cl2, RT, 1 h View Scheme
参考文献
Rathore, Hargovind; From, Arthur H. L.; Ahmed, Khalil; Fullerton, Dwight S.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 10 p. 1945 - 1952
反应条件
Multi-step reaction with 2 steps 1: 100 percent / NaOMe / methanol / 2 h2: PCC; 4 Angstroem molecular sieves / CH2Cl2 / 2 h / 0 °C
参考文献
Wang, Wei; Zhang, Yongmin; Sollogoub, Matthieu; Sinay, Pierre Angewandte Chemie (International Edition in English), 2000 , vol. 39, # 14 p. X2466-2467
