1-(4-(3,5-二甲基苯氧基)苯基)乙酮合成路线 (共 3 条)
反应条件
anhydrous iron chloride; 2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate in N,N-dimethyl-formamide
T=135°C; 24 h; Inert atmosphere;
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (C.N.R.S)
Patent: US2011/306782 A1, 2011 ;
Location in patent: Page/Page column 13 ;
反应条件
2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate; copper(I) bromide in N,N-dimethyl-formamide
T=135°C; 36 h; Inert atmosphere;
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (C.N.R.S)
Patent: US2011/306782 A1, 2011 ;
Location in patent: Page/Page column 13 ;
反应条件
caesium carbonate in N,N-dimethyl-formamide
T=145°C; 24 h; Inert atmosphere;
参考文献
Pichette Drapeau, Martin; Ollevier, Thierry; Taillefer, Marc
Chemistry - A European Journal, 2014 , vol. 20, # 18 p. 5231 - 5236