5-(1-甲基-1H-苯并咪唑-2-基)-2-糠醛合成路线 （共 6 条）
反应条件
1: With potassium dichromate; sulfuric acid in water T=80°C; 2: With ammonia in water
参考文献
Aleksandrov; Savost'yanov; El'chaninov; Salamatina
Russian Journal of General Chemistry, 2011 , vol. 81, # 8 p. 1716 - 1719
反应条件
1: [13C]-Caffeine With pyridine; palladium diacetate; copper (II) acetate monohydrate in 1,4-dioxane
T=20°C; 0.166667 h; Inert atmosphere;
2: furfural in 1,4-dioxane
T=120°C; 20 h; Inert atmosphere;
参考文献
Xi, Peihua; Yang, Fan; Qin, Song; Zhao, Dongbing; Lan, Jingbo; Gao, Ge; Hu, Changwei; You, Jingsong
Journal of the American Chemical Society, 2010 , vol. 132, # 6 p. 1822 - 1824
反应条件
selenium(IV) oxide in 1,4-dioxane
20 h; Heating;
参考文献
El'chaninov, M. M.; Simonov, A. M.; Simkin, B. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 8 p. 833 - 835
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 8 p. 1089 - 1091
参考文献
El'chaninov, M. M.; Simonov, A. M.; Oleinikova, L. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , p. 1041 - 1043
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 10 p. 1311 - 1313
反应条件
n-butyllithium
1.) ether, hexane, 0 deg C, 15 min, 2.) ether, hexane, from 0 deg C to RT; Yield given. Multistep reaction;
参考文献
Stoyanov, V. M.; El'chaninov, M. M.; Pozharskii, A. F.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 1 p. 53 - 57
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 1 p. 61 - 66
反应条件
n-butyllithium
1.) ether, hexane, -70 deg C, 1 h, 2.) ether, hexane, from -70 deg C to RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Stoyanov, V. M.; El'chaninov, M. M.; Pozharskii, A. F.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 1 p. 53 - 57
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 1 p. 61 - 66
