4-氯-5,6-二甲基-2-苯基噻吩并[2,3-d]嘧啶合成路线 （共 4 条）
反应条件
trichlorophosphate in 1,4-dioxane
3 h; Heating;
参考文献
Prasad, Mailavaram Raghu; Rao, Akkinepalli Raghu Ram; Rao, Pamulaparthi Shanthan; Rajan, Kombu Subramanian
Synthesis, 2001 , # 14 p. 2119 - 2123
反应条件
1: HCl / dioxane / 3 h
2: POCl3 / dioxane / 3 h / Heating
View Scheme
参考文献
Prasad, Mailavaram Raghu; Rao, Akkinepalli Raghu Ram; Rao, Pamulaparthi Shanthan; Rajan, Kombu Subramanian
Synthesis, 2001 , # 14 p. 2119 - 2123
反应条件
1: neat (no solvent) / |Microwave irradiation
2: trichlorophosphate / |Reflux
View Scheme
参考文献
Sanchez, Ana I.; Meneses, Ricardo; Minguez, Jose M.; Nunez, Araceli; Castillo, Rafael R.; Filace, Fabiana; Burgos, Carolina; Vaquero, Juan J.; Alvarez-Builla, Julio; Cortes-Cabrera, Alvaro; Gago, Federico; Terricabras, Emma; Segarra, Victor
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 24 p. 4233 - 4242
反应条件
1: HCl / dioxane / 3 h
2: POCl3 / dioxane / 3 h / Heating
View Scheme
参考文献
Prasad, Mailavaram Raghu; Rao, Akkinepalli Raghu Ram; Rao, Pamulaparthi Shanthan; Rajan, Kombu Subramanian
Synthesis, 2001 , # 14 p. 2119 - 2123
