(S)-2-吡啶硫代半胱胺盐酸盐合成路线 （共 4 条）
反应条件
hydrogenchloride; water in ethyl acetate
T=20°C; 0.5 h;
参考文献
IMMUNOGEN, INC.; LI, Wei; FISHKIN, Nathan, Elliott; ZHAO, Robert, Yongxin; MILLER, Michael, Louis; CHARI, Ravi, V., J.
Patent: WO2010/91150 A1, 2010 ;
Location in patent: Page/Page column 152-153 ;
反应条件
1: in methanol
T=20°C; 21 h;
2: With triethylamine in methanol
参考文献
IMMUNOGEN, INC.; LI, Wei; FISHKIN, Nathan, Elliott; ZHAO, Robert, Yongxin; MILLER, Michael, Louis; CHARI, Ravi, V., J.
Patent: WO2010/91150 A1, 2010 ;
Location in patent: Page/Page column 134 ;
参考文献
Cui, Zhiyong; Sun, Lele; Zhang, Biliang
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 5 p. 927 - 933
反应条件
in methanol
T=20°C; 1.5 h;
参考文献
Daly, Trevor A.; Almeida, Paulo F.; Regen, Steven L.
Journal of the American Chemical Society, 2012 , vol. 134, # 41 p. 17245 - 17252
