2-氨基甲基-15-冠-5合成路线 （共 7 条）
反应条件
sodium t-butanolate in 1,4-dioxane; tert-butyl alcohol T=40°C; 2.5 h;
参考文献
Maeda, Hirokazu; Kikui, Takashi; Nakatsuji, Yohji; Okahara, Mitsuo
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5167 - 5171
反应条件
1: 53 percent / 26percent aq. NH3, K2CO3 / 55 h / Ambient temperature 2: 53 percent / tert-BuONa / dioxane; 2-methyl-propan-2-ol / 2.5 h / 40 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 26 p. 5167 - 5171
参考文献
Journal of Organic Chemistry, , vol. 47, # 26 p. 5167 - 5171
反应条件
1: 70 percent / diethylazodicarboxylate, triphenylphosphine / tetrahydrofuran / 10 h / Ambient temperature 2: hydrazine hydrate / methanol / 1 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 25, # 11 p. 1107 - 1110
反应条件
hydrazine hydrate in methanol 1 h; Heating;
参考文献
Tetrahedron Letters, , vol. 25, # 11 p. 1107 - 1110
反应条件
1: 90 percent / dimethylformamide / 7 h / Heating 2: hydrazine hydrate / methanol / 1 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 25, # 11 p. 1107 - 1110
反应条件
1: 43 percent / 26percent aq. NH3, K2CO3 / 55 h / Ambient temperature 2: 41 percent / tert-BuONa View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 26 p. 5167 - 5171
