2-氨基甲基-18-冠-6合成路线 （共 5 条）
反应条件
sodium t-butanolate in 1,4-dioxane; tert-butyl alcohol
T=40°C; 2.5 h;
参考文献
Maeda, Hirokazu; Kikui, Takashi; Nakatsuji, Yohji; Okahara, Mitsuo
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5167 - 5171
反应条件
sodium t-butanolate in 1,4-dioxane; tert-butyl alcohol
T=40°C; 2.5 h;
参考文献
Maeda, Hirokazu; Kikui, Takashi; Nakatsuji, Yohji; Okahara, Mitsuo
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5167 - 5171
反应条件
1: 53 percent / 26percent aq. NH3, K2CO3 / 55 h / Ambient temperature
2: 43 percent / tert-BuONa / dioxane; 2-methyl-propan-2-ol / 2.5 h / 40 °C
View Scheme
参考文献
Maeda, Hirokazu; Kikui, Takashi; Nakatsuji, Yohji; Okahara, Mitsuo
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5167 - 5171
反应条件
1: 43 percent / 26percent aq. NH3, K2CO3 / 55 h / Ambient temperature
2: 40 percent / tert-BuONa / dioxane; 2-methyl-propan-2-ol / 2.5 h / 40 °C
View Scheme
参考文献
Maeda, Hirokazu; Kikui, Takashi; Nakatsuji, Yohji; Okahara, Mitsuo
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5167 - 5171
反应条件
hydrazine hydrate in ethanol
3 h; Heating; Yield given;
参考文献
Anelli, Pier Lucio; Montanari, Fernando; Pollak, Vladimir; Quici, Silvio
Gazzetta Chimica Italiana, 1986 , vol. 116, # 3 p. 127 - 132
